[1] Carrao D B, Perovani I S, De Albuquerque N C P, et al. Enantioseparation of pesticides: acritical review[J]. Trac-Trends in Analytical Chemistry, 2020, 122: 115719. doi: 10.1016/j.trac.2019.115719.
[2] Zhong Q, Li H X, Wang M, et al.Enantioselectivity of indoxacarb during the growing, processing, and brewing of tea: degradation, metabolites, and toxicities[J]. Science of the Total Environment, 2022, 823: 153763. doi: 10.1016/j.scitotenv.2022.153763.
[3] Zhang X Z, Wang X R, Luo F J, et al.Application and enantioselective residue determination of chiral pesticide penconazole in grape, tea, aquatic vegetables and soil by ultra performance liquid chromatography-tandem mass spectrometry[J]. Ecotoxicology and Environmental Safety, 2019, 172: 530-537.
[4] 李子璇, 杨雪葳, 任利翔, 等. 有机氯农药介导的内分泌干扰相关不良结局通路(AOP)的研究进展[J]. 农药, 2021, 60(10): 703-711.
Li Z X, Yang X W, Ren L X, et al.Advances in studies on endocrine disruption-related adverse outcome pathways (AOP) mediated by organochlorine pesticides[J]. Agrochemicals, 2021, 60(10): 703-711.
[5] 席北斗, 虞敏达, 张媛, 等. 华北典型污灌区有机氯农药残留特征及健康风险评价[J]. 生态毒理学报, 2016, 11(2): 453-464.
Xi B D, Yu M D, Zhang Y, et al.Residues and health risk assessments of organochlorine pesticides in a typical wastewater irrigation area of North China[J]. Asian Journal of Ecotoxicology, 2016, 11(2): 453-464.
[6] 农药信息网. 禁限用农药名录[EB/OL]. (2022-09-01) [2024-03-08]. http://www.chinapesticide.org.cn/zgnyxxw/zwb/detail/13081.China Pesticide Information Network. List of banned and restricted pesticides [EB/OL]. (2022-09-01) [2024-03-08]. http://www.chinapesticide.org.cn/zgnyxxw/zwb/detail/13081.
[7] Tsai Y, Lein P J.Mechanisms of organophosphate neurotoxicity[J]. Current Opinion in Toxicology, 2021, 26: 49-60.
[8] Lin K D, Zhou S S, Xu C, et al.Enantiomeric resolution and biotoxicity of methamidophos[J]. Journal of Agricultural and Food Chemistry, 2006, 54(21): 8134-8138.
[9] 李雪妍. 两种拟除虫菊酯类手性农药对大型蚤的对映体选择性毒理研究[D]. 泉州: 华侨大学, 2019.
Li X Y.Study on selective enantiomeric toxicology of two chiral pesticides of pyrethroids on Daphnia magna [D]. Quanzhou: Huaqiao University, 2019.
[10] 李玲, 李俊杰, 王俊英, 等. 手性农药水胺硫磷对浮游生物氧化应激的对映体选择性影响[J]. 生态毒理学报, 2021, 16(3): 264-272.
Li L, Li J J, Wang J Y, et al.Enantiomeric selectivity of chiral pesticide isocarbophos on oxidative stress in plankton[J]. Asian Journal of Ecotoxicology, 2021, 16(3): 264-272.
[11] Coats J R.Mechanisms of toxic action and structure-activity relationships for organochlorine and synthetic pyrethroid insecticides[J]. Environmental Health Perspectives, 1990, 87: 255-262.
[12] 王鹏, 周志强. 手性农药手册[M]. 北京: 化学工业出版社, 2021.
Wang P, Zhou Z Q.Book of chiral pesticides [M]. Beijing: Chemical Industry Press, 2021.
[13] 熊康. 溴敌隆、氰戊菊酯和哌虫啶三种农药对蚯蚓的毒性和生物富集研究[D]. 杭州: 浙江大学, 2015.
Xiong K.Toxicity and bioaccumulation of bromadiolone, fenvalerate and paichongding to earthworm Eisenia fetida [D]. Hangzhou: Zhejing University, 2015.
[14] 崔璇. 在线SPE-UPLC-MS/MS建立茶叶中4种拟除虫菊酯类农药检测方法及高效氯氟氰菊酯对茶尺蠖的活性差异[D]. 天津: 天津农学院, 2019.
Cui X.Online SPE-UPLC-MS/MS to establish four pyrethroid pesticides in tea and lambda-cyhalothrin activity differences of Ectropis oblique hypulina Wehrli [D]. Tianjin: Tianjin Agricultural University, 2019.
[15] Zhou C H, Wang Y.Recent researches in triazole compounds as medicinal drugs[J]. Current Medicinal Chemistry, 2012, 19(2): 239-280.
[16] 杨森. 三唑类杀菌剂作用机理和残留检测技术分析研究[J]. 农药科学与管理, 2020, 41(6): 27-32.
Yang S.Study on the mechanism and residue detection technology of triazole fungicides[J]. Pesticide Science and Administration, 2020, 41(6): 27-32.
[17] Vieira A C, Santos M G, Figueiredo E C.Solid-phase extraction of triazole fungicides from water samples using disks impregnated with carbon nanotubes followed by GC-MS analysis[J]. International Journal of Environmental Analytical Chemistry, 2017, 97(1): 29-41.
[18] 陈茜茜. 戊唑醇手性杀菌剂在拟南芥中的选择性降解及其机制研究[D]. 北京: 中国农业科学院, 2016.
Chen Q Q.Studies on the stereoselectivity degradation and its mechanism of chiral fungicide tebuconazole in Arabidopsis thaliana [D]. Beijing: Chinese Academy of Agricultural Sciences, 2016.
[19] Zhang A P, Xie X M, Liu W P.Enantioselective separation and phytotoxicity on rice seedlings of paclobutrazol[J]. Journal of Agricultural and Food Chemistry, 2011, 59(8): 4300-4305.
[20] 贺敏. 苯醚甲环唑手性异构体活性差异及其在稻田的立体环境行为[D]. 北京: 中国农业科学院, 2017.
He M.Bioactivity difference of difenoconazole stereoisomers and their stereooselective environmental behavior in paddy field [D]. Beijing: Chinese Academy of Agricultural Sciences, 2017.
[21] 刘子琪, 呼啸, 李莉, 等. 新烟碱类农药呋虫胺对映体选择性研究进展[J]. 中国环境科学, 2021, 41(10): 4811-4819.
Liu Z Q, Hu X, Li L, et al.Research progress on the enantioselectivity of a neonicotinoid pesticide dinotefuran[J]. China Environmental Science, 2021, 41(10): 4811-4819.
[22] 绳慧珊. 呋虫胺对映体在茶叶中的残留降解行为及对茶尺蠖的活性差异研究[D]. 天津: 天津农学院, 2018.
Sheng H S.The residue of dinotefuran enantiomers in tea and their activity differences of tea geometrid [D]. Tianjin: Tianjin Agricultural University, 2018.
[23] 周佳, 梁水连, 相坛坛, 等. 手性农药研究进展[J]. 江西农业学报, 2021, 33(7): 75-80.
Zhou J, Liang S L, Xiang T T, et al.Research progress in chiral pesticides[J]. Acta Agriculturae Jiangxi, 2021, 33(7): 75-80.
[24] 王鹏, 江树人, 张宏军, 等. 戊唑醇和三唑酮对映体的手性拆分[J]. 分析化学, 2004, 32(5): 625-627.
Wang P, Jiang S R, Zhang H J, et al.The enantiomeric separation of tebuconazole and triadimefon[J]. Chinese Journal of Analytical Chemistry, 2004, 32(5): 625-627.
[25] 田芹, 任丽萍, 吕春光, 等. 反相色谱条件下三唑类手性农药对映异构体的拆分[J]. 分析化学, 2010, 38(5): 688-692.
Tian Q, Ren L P, Lü C G, et al.Chiral resolution of eight triazole pestioioles by high performance liquid chromatography under reversed phase conditions[J]. Chinese Journal of Analytical Chemistry, 2010, 38(5): 688-692.
[26] Kuang H, Miao H, Hou X L, et al.Determination of enantiomeric fractions of cypermethrin and cis-bifenthrin in Chinese teas by GC/ECD[J]. Journal of the Science of Food and Agriculture, 2010, 90(8): 1374-1379.
[27] Wang X Y, Zhang H, Xu H, et al.Direct chiral determination of acephate and its metabolite methamidophos in vegetables using QuEChERS by gas chromatography-tandem mass spectrometry[J]. Food Analytical Methods, 2013, 6(1): 133-140.
[28] 宁亚婷, 王新茹, 罗逢健, 等. 茶叶和土壤中cis-联苯菊酯、高效氯氟氰菊酯手性对映体残留分析[J]. 核农学报, 2023, 37(11): 2243-2251.
Ning Y T, Wang X R, Luo F J, et al.Enantioseparation and residue analysis of cis-bifenthrin and lambda-cyhalothrin in tea and soil[J]. Journal of Nuclear Agricultural Sciences, 2023, 37(11): 2243-2251.
[29] 冯硕立, 徐明仙, 高伟亮, 等. 超临界色谱拆分6种唑类手性农药[J]. 浙江工业大学学报, 2011, 39(4): 424-428.
Feng S L, Xu M X, Gao W L, et al.Enantiomer resolution of six triazole with supercritical fluid chromatography[J]. Journal of Zhejiang University of Technology, 2011, 39(4): 424-428.
[30] 缪叶隆. 含硫/磷农药的超临界流体色谱手性分离及体外降解研究[D]. 杭州: 浙江工业大学, 2020.
Miao Y L.Eenantiomer separation and stereoselective metabolism in vitro of chiral pesticides containing S/P [D]. Hangzhou: Zhejiang University of Technology, 2020.
[31] 张天赐, 钟慧, 双亚洲, 等. 高效液相色谱法测定苹果和西红柿中腈菌唑对映体含量[J]. 分析科学学报, 2021, 37(3): 273-278.
Zhang T C, Zhong H, Shuang Y Z, et al.Determination of myclobutanil rnantiomers in apples and tomatoes by high performance liquid chromatography[J]. Journal of Analytical Science, 2021, 37(3): 273-278.
[32] 张文华, 谢文, 侯建波, 等. 超高效合相色谱法对6种三唑类农药对映体的拆分及其在黄瓜中的残留分析[J]. 色谱, 2019, 37(12): 1356-1362.
Zhang W H, Xie W, Hou J B, et al.Chiral separation of six triazole pesticide enantiomers by ultra-performance convergence chromatography and residue determination in cucumber[J]. Chinese Journal of Chromatography, 2019, 37(12): 1356-1362.
[33] 周励, 唐婧, 范荣华, 等.反相高效液相色谱法同时拆分3种手性杀菌剂[J/OL]. 分析试验室, 2023[2024-03-08]. https://doi.org/10.13595/j.cnki.issn1000-0720.2023.041301.
Zhou L, Tang J, Fan R H, et al.Simultaneous enantiomeric separation of three triazole fungicides by reversed-phase high performance liquid chromatography [J/OL]. Chinese Journal of Analysis Laboratory, 2023 [2024-03-08]. https://doi.org/10.13595/j.cnki.issn1000-0720.2023.041301.
[34] 胡建华, 姚华珍, 周珊珊, 等. 高效液相色谱法拆分手性农药及其热力学研究[J]. 农药, 2008, 47(8): 590-592.
Hu J H, Yao H Z, Zhou S S, et al.Enantioseparation and study of thermodynamical property of chiral pesticdes by HPLC[J]. Agrochemicals, 2008, 47(8): 590-592.
[35] 齐艳丽, 李晋栋, 吕莹, 等. 超高效合相色谱法对9种三唑类手性农药对映体的分离分析[J]. 农药, 2023, 62(6): 422-427.
Qi Y L, Li J D, Lü Y, et al.Enantiomer separation and analysis of 9 chiral pesticides by ultra performance convergence chromatography[J]. Agrochemicals, 2023, 62(6): 422-427.
[36] 曾皓鹏, 雷红涛, 张炽坚, 等. 手性农药兽药免疫分析研究进展[J]. 食品科学, 2014, 35(21): 315-321.
Zeng H P, Lei H T, Zhang C J, et al.Advances in immunoassay of chiral pesticides and veterinary drugs[J]. Food Science, 2014, 35(21): 315-321.
[37] 郑依柳, 邵华, 金芬, 等. 分子印迹材料在手性拆分中的应用研究进展[J]. 化学试剂, 2024, 46(2): 47-54.
Zheng Y L, Shao H, Jin F, et al.Research progress on applications of molecularly imprinted materials in chiral discrimination[J]. Chemical Reagents, 2024, 46(2): 47-54.
[38] 陈丹丹, 万建春, 郭平, 等. 植物源性食品中手性农药残留检测技术的研究进展[J]. 江西农业学报, 2021, 33(9): 100-108.
Chen D D, Wan J C, Guo P, et al.Research progress in detection of chiral pesticide residues in plant-derived food[J]. Acta Agriculturae Jiangxi, 2021, 33(9): 100-108.
[39] Zheng X J, Ma W W, Wang Q H, et al.Development of self-dispersion ferrofluid-based dispersive liquid-liquid microextraction for determining chiral fungicide hexaconazole in water, tea, and juice using high-performance liquid chromatography[J]. Microchemical Journal, 2024, 196: 109593. doi: 10.1016/j.microc.2023.109593.
[40] Inoue K, Prayoonhan N, Tsutsui H, et al.Use of chiral derivatization for the determination of dichlorprop in tea samples by ultra performance LC with fluorescence detection: liquid chromatography[J]. Journal of Separation Science, 2013, 36(8): 1356-1361.
[41] Liu H C, Lin T, Li Q W.Development and validation of multiclass chiral pesticide residues analysis method in tea by quechers combined liquid chromatography quadruple-linear ion trap mass spectrometry[J]. Journal of Aoac International, 2020, 103(3): 865-871.
[42] 蒋明明, 曾小娟, 宋红坤, 等. 多壁碳纳米管/N-丙基乙二胺混合吸附-超高效液相色谱-串联质谱法测定普洱茶中3种手性杀菌剂农药残留[J]. 食品安全质量检测学报, 2020, 11(6): 1702-1708.
Jiang M M, Zeng X J, Song H K, et al.Determination of 3 chiral fungicide pesticide residues in Pu-erh tea by multiwalled carbon nanotubes/primary secondary amine mixed adsorption-ultra performance liquid chromatography-tandem mass spectrometry[J]. Journal of Food Safety and Quality, 2020, 11(6): 1702-1708.
[43] 曾小娟, 林涛, 王莉丽, 等. QuEChERS-超高效液相色谱-串联质谱法测定茶叶中3种杀虫剂手性农药[J]. 食品安全质量检测学报, 2021, 12(2): 602-608.
Zeng X J, Lin T, Wang L L, et al.Determination of 3 kinds of chiral pesticides in tea by QuEChERS-ultra performance liquid chromatography-tandem mass spectrometry[J]. Journal of Food Safety and Quality, 2021, 12(2): 602-608.
[44] 武杨柳, 李栋, 康露, 等. 质谱技术在农药残留分析中的研究进展[J]. 质谱学报, 2021, 42(5): 691-708.
Wu Y L, Li D, Kang L, et al.Research progress of mass spectrometry in pesticide residue analysis[J]. Journal of Chinese Mass Spectrometry Society, 2021, 42(5): 691-708.
[45] Zhang X Z, Luo F J, Lou Z Y, et al.Simultaneous and enantioselective determination of cis-epoxiconazole and indoxacarb residues in various teas, tea infusion and soil samples by chiral high performance liquid chromatography coupled with tandem quadrupole-time-of-flight mass spectrometry[J]. Journal of Chromatography A, 2014, 1359: 212-223.
[46] 张新忠, 罗逢健, 陈宗懋, 等. 超高效液相色谱-四极杆飞行时间质谱测定茶叶中手性农药茚虫威对映体残留[J]. 质谱学报, 2012, 33(6): 321-326.
Zhang X Z, Luo F J, Chen Z M, et al.Enantioseparation and quantification of chiral pesticide indoxacarb residues in tea by UHPLC-Q-TOF/MS[J]. Journal of Chinese Mass Spectrometry Society, 2012, 33(6): 321-326.
[47] Liu H C, Jiang M M, Li Q W.Determination of neonicotinoid sulfoxaflor residues and stereoselective degradation in Pu-erh tea and black tea by liquid chromatography-high-resolution mass spectrometry[J]. Journal of Food Processing and Preservation, 2020, 44(8): e14589. doi: 10.1111/jfpp.14589.
[48] Chen H P, Gao G W, Yin P, et al.Enantioselectivity and residue analysis of fipronil in tea (Camellia sinensis) by ultra-performance liquid chromatography orbitrap mass spectrometry[J]. Food Additives & Contaminants: Part A, 2018, 35(10): 2000-2010.
[49] Liu H, Li P Z, Wang P, et al.Toxicity risk assessment of pyriproxyfen and metabolites in the rat liver: a vitro study[J]. Journal of Hazardous Materials, 2020, 389: 121835. doi: 10.1016/j.jhazmat.2019.121835.
[50] Liu H C, Tian H, Jiang M M, et al.Enantioselectivity and residue analysis of cycloxaprid and its metabolite in the pile and fermentation processing of Puer tea by ultraperformance liquid chromatography-high-resolution mass spectrometry[J]. Food Science & Nutrition, 2022, 10(9): 3043-3051.
[51] Zhang X Z, Sun H Z, Wang X R, et al.Enantioselective residue analysis of oxathiapiprolin and its metabolite in tea and other crops by ultra-high performance liquid chromatography-tandem mass spectrometry[J]. Journal of Separation Science, 2020, 43(20): 3856-3867.
[52] 钟青, 黎洪霞, 罗逢健, 等. 超高效液相色谱-串联质谱法测定茶叶和茶汤中茚虫威对映体及7种降解产物[J]. 质谱学报, 2021, 42(2): 140-153.
Zhong Q, Li H X, Luo F J, et al.Analysis of indoxacarb enantiomers and its seven metabolites in tea and tea infusion by ultra performance liquid chromatography tandem triple quadrupole mass spectrometry[J]. Journal of Chinese Mass Spectrometry Society, 2021, 42(2): 140-153.
[53] 潘蓉, 陈红平, 尹鹏, 等. 茶叶中乙酰甲胺磷及甲胺磷对映体的气相色谱法分离与测定[J]. 分析测试学报, 2014, 33(7): 766-772.
Pan R, Chen H P, Yin P, et al.Direct isolation and determination of acephate and methamidophos enantiomers in tea by gas chromatography[J]. Journal of Instrumental Analysis, 2014, 33(7): 766-772.
[54] Jiao W T, Hou R Y, Li J C, et al.Enantiomer metabolism of acephate and its metabolite methamidophos in in vitro tea (Camellia sinensis L.) systems: comparison between cell suspensions and excised tissues[J]. Science of the Total Environment, 2022, 806: 150863. doi: 10.1016/j.scitotenv.2021.150863.
[55] 刘培培, 杨继远, 郭全海. 毛细管电泳和毛细管电色谱技术在农药残留检测中的应用[J]. 农业技术与装备, 2022(3): 70-72.
Liu P P, Yang J Y, Guo Q H.Application of capillary electrophoresis and capillary electrochromatography in the detection of pesticide residues[J]. Agricultural Technology & Equipment, 2022(3): 70-72.
[56] García-Ruiz C, Álvarez-Llamas G, Puerta Á, et al.Enantiomeric separation of organophosphorus pesticides by capillary electrophoresis[J]. Analytica Chimica Acta, 2005, 543(1/2): 77-83.
[57] Jarman J L, Jones W J, Howell L A, et al.Application of capillary electrophoresis to study the enantioselective transformation of five chiral pesticides in aerobic soil slurries[J]. Journal of Agricultural and Food Chemistry, 2005, 53(16): 6175-6182.
[58] Lewis D L, Garrison A W, Wommack K E, et al.Influence of environmental changes on degradation of chiral pollutants in soils[J]. Nature, 1999, 401(6756): 898-901.
[59] Gogolashvili A, Tatunashvili E, Chankvetadze L, et al.Separation of enilconazole enantiomers in capillary electrophoresis with cyclodextrin-type chiral selectors and investigation of structure of selector-selectand complexes by using nuclear magnetic resonance spectroscopy[J]. Electrophoresis, 2017, 38(15): 1851-1859.
[60] Pérez-Fernández V, García M Á, Marina M L.Enantiomeric separation of cis-bifenthrin by CD-MEKC: quantitative analysis in a commercial insecticide formulation[J]. Electrophoresis, 2010, 31(9): 1533-1539.
[61] 李佳, 任晓慧, 冯涛, 等. 精喹禾灵与其S-对映体的高效毛细管电泳手性分离方法[J]. 农药, 2014, 53(3): 189-190.
Li J, Ren X H, Feng T, et al.Separation and analysis of quizalofop-p-ethyl and S-enantiomer by high performance capillary electrophoresis[J]. Agrochemicals, 2014, 53(3): 189-190.
[62] Yi F, Guo B Y, Peng Z L, et al.Study of the enantioseparation of imazaquin and enantioselective degradation in field soils by CZE[J]. Electrophoresis, 2007, 28(15): 2710-2716.
[63] 王丽. 基于QuEChERS-超临界流体色谱-串联质谱法的茶叶中甲胺磷及乙酰甲胺磷对映体拆分及定量[J]. 安徽农业科学, 2023, 51(11): 156-162.
Wang L.Separation and quantification of methamidophos and acephate enantiomer in tea based on QuEChERS-supercritical fluid chromatography-tandem mass spectrometry[J]. Journal of Anhui Agricultural Sciences, 2023, 51(11): 156-162.
[64] Zhang X Z, Zhao Y C, Cui X Y, et al. Application and enantiomeric residue determination of diniconazole in tea and grape and apple by supercritical fluid chromatography coupled with quadrupole-time-of-flight mass spectrometry [J]. Journal of Chromatography A, 2018, 1581/1582: 144-155.
[65] 赵悦臣, 张新忠, 罗逢健, 等. 超高效合相色谱-四极杆飞行时间质谱法测定水果和茶叶中手性农药顺式-氟环唑对映体残留[J]. 分析化学, 2016, 44(8): 1200-1208.
Zhao Y C, Zhang X Z, Luo F J, et al.Residue determination of cis-epoxiconazole enantiomers in fruit and tea by ultra performance convergence chromatography combined with quadrupole time-of-flight mass spectrometry[J]. Chinese Journal of Analytical Chemistry, 2016, 44(8): 1200-1208.
[66] 赵悦臣. 水果和茶叶中四种手性农药对映体多残留分析方法研究[D]. 天津: 天津农学院, 2016.
Zhao Y C.The research of multiple residue analysis of four chiral pesticides in fruit and tea [D]. Tianjin: Tianjin Agricultural University, 2016.
[67] 张新忠, 赵悦臣, 罗逢健, 等. 水果和红茶中腈菌唑对映体残留的超高效合相色谱四极杆飞行时间质谱分析[J]. 分析测试学报, 2016, 35(11): 1376-1383.
Zhang X Z, Zhao Y C, Luo F J, et al.Determination of myclobutanil enantiomers residues in fruit and black tea samples by ultra performance convergence chromatography quadrupole time-of-flight mass spectrometry[J]. Journal of Instrumental Analysis, 2016, 35(11): 1376-1383.
[68] Gupta M, Shanker A.Fate of imidacloprid and acetamiprid residues during black tea manufacture and transfer into tea infusion[J]. Food Additives & Contaminants: Part A, 2009, 26(2): 157-163.
[69] Paramasivam M, Deepa M, Selvi C, et al.Dissipation kinetics of beta-cyfluthrin and imidacloprid in tea and their transfer from processed tea to infusion[J]. Ecotoxicology and Environmental Safety, 2017, 144: 531-536.
[70] Kumar V, Ravindranath S D, Shanker A.Fate of hexaconazole residues in tea and its behavior during brewing process[J]. Chemical Health & Safety, 2004, 11(1): 21-25.
[71] 李红莉, 毛宇骁, 敖存, 等. 不同覆盖条件下3种农药在抹茶中的消解动态比较[J]. 现代农药, 2022, 21(1): 53-56.
Li H L, Mao Y X, Ao C, et al.Degradation dynamics comparison of three pesticides applied to matcha under different coverage conditions[J]. Modern Agrochemicals, 2022, 21(1): 53-56.
[72] 潘蓉. 三种农药在茶叶种植-加工过程中的消解动态及其在茶汤中的浸出率[D]. 北京: 中国农业科学院, 2015.
Pan R.Dissipation behavior of three pesticides during tea cultivation and manufacturing, and their transfer in tea brewing [D]. Beijing: Chinese Academy of Agricultural Sciences, 2015.
[73] Pan R, Chen H P, Wang C, et al.Enantioselective dissipation of acephate and its metabolite, methamidophos, during tea cultivation, manufacturing, and infusion[J]. Journal of Agricultural and Food Chemistry, 2015, 63(4): 1300-1308.
[74] 黎洪霞. 吡丙醚在茶叶中的残留降解研究[D]. 北京: 中国农业科学院, 2021.
Li H X.Study on residue degradation of pyriproxyfen in tea [D]. Beijing: Chinese Academy of Agricultural Sciences, 2021.
[75] Zhang Y P, Hu D Y, Meng X G, et al.Enantioselective degradation of indoxacarb from different commercial formulations applied to tea[J]. Chirality, 2015, 27(3): 262-267.
[76] Wang M, Li Y J, Wang X R, et al.Enantioselective residue dissipation of oxathiapiprolin during tea growing, processing, and brewing[J]. Acs Agricultural Science & Technology, 2022, 2(5): 969-979.
[77] 杨佳洁, 李敏敏, 肖欧丽, 等. 果蔬加工过程农药残留行为研究及加工因子在风险评估中的应用[J]. 食品安全质量检测学报, 2022, 13(22): 7255-7263.
Yang J J, Li M M, Xiao O L, et al.Study on pesticide residue behavior during fruit and vegetable processing and application of processing factors in risk assessment[J]. Journal of Food Safety and Quality, 2022, 13(22): 7255-7263.
[78] 李晓刚, 刘一平, 刘双清, 等. 茚虫威对映体在土壤中的选择性降解[J]. 环境化学, 2012, 31(8): 1262-1267.
Li X G, Liu Y P, Liu S Q, et al.Enantioselective degradation of indoxacarb enantiomers in soils[J]. Environmental Chemistry, 2012, 31(8): 1262-1267.
[79] 陈增龙. 呋虫胺对映体选择性环境行为与毒性差异分子机制[D]. 北京: 中国农业科学院, 2017.
Chen Z L.Enantionselective environmental fate and chiralspecific molecular toxicology of finotefuran [D]. Beijing: Chinese Academy of Agricultural Sciences, 2017.
[80] 薛鹏飞, 刘潇威, 赵刘清, 等. 手性三唑类杀菌剂氟环唑对土壤微生物的立体选择性影响[J]. 农业环境科学学报, 2022, 41(6): 1284-1295.
Xue P F, Liu X W, Zhao L Q, et al.Study on pesticide residue behavior during fruit and vegetable processing and application of processing factors in risk assessment[J]. Journal of Agro-Environment Science, 2022, 41(6): 1284-1295.
[81] 张芬, 张新忠, 罗逢健, 等. QuEChERS净化GC/ECD测定茶叶与土壤中噻虫嗪、虫螨腈及高效氯氟氰菊酯残留[J]. 分析测试学报, 2013, 32(4): 393-400.
Zhang F, Zhang X Z, Luo F J, et al.Residue analysis of thiamethoxam, chlorfenapyr and lambda-cyhalothrin in tea and soil by GC/ECD after QuEChERS clean-up[J]. Journal of Instrumental Analysis, 2013, 32(4): 393-400.
[82] Kumar V, Sood C, Jaggi S, et al.Dissipation behavior of propargite: an acaricide residues in soil, apple (Malus pumila) and tea (Camellia sinensis)[J]. Chemosphere, 2005, 58(6): 837-843.
[83] Bishnu A, Saha T, Mazumdar D, et al.Assessment of the impact of pesticide residues on microbiological and biochemical parameters of tea garden soils in India[J]. Journal of Environmental Science and Health, Part B, 2008, 43(8): 723-731.
[84] 刘新, 陈红平, 王国庆. 中国茶叶质量安全40年[J]. 中国茶叶, 2019, 41(12): 1-9.
Liu X, Chen H P, Wang G Q.40 years of tea quality and safety in China[J]. China Tea, 2019, 41(12): 1-9.
[85] 佚名. 食品中农药残留风险评估指南[J]. 农村实用技术, 2016(2): 10-11.
Anon. Guidelines for risk assessment of pesticide residues in food[J]. Journal of Rural Practical Technology, 2016(2): 10-11.
[86] 郭浩铭, 魏一木, 刘雪科, 等. 手性农药选择性生物活性与毒性效应研究进展[J]. 农药学学报, 2022, 24(5): 1108-1124.
Guo H M, Wei Y M, Liu X K, et al.Research progress on the stereoselective bioactivity and toxicity of chiral pesticides[J]. Chinese Journal of Pesticide Science, 2022, 24(5): 1108-1124.
[87] 石琳琳, 杨灿灿, 陈琪, 等. 丁氟螨酯在蚯蚓体内的富集及其急性毒性[J]. 农药学学报, 2022, 24(1): 177-181.
Shi L L, Yang C C, Chen Q, et al.Accumulation and acute toxicity of cyflumetofen in earthworms[J]. Chinese Journal of Pesticide Science, 2022, 24(1): 177-181.
[88] 刘思宏. 呋虫胺对映体对蜜蜂的亚致死效应研究[D]. 南宁: 广西大学, 2018.
Liu S H.Sublethal effects of dinotefuran enantiosmers on honeybees Apis mellifera L. [D]. Nanning: Guangxi University, 2018.
[89] Liu T, Chen D, Li Y Q, et al.Enantioselective bioaccumulation and toxicity of the neonicotinoid insecticide dinotefuran in earthworms ( Eisenia fetida )[J]. Journal of Agricultural and Food Chemistry, 2018, 66(17): 4531-4540.
[90] 夏玮彤. 仲丁威对映体立体选择性生物效应和降解研究[D]. 南京: 南京农业大学, 2019.
Xai W T.Studies on enantioselective biological effect and degradation of fenobucarb enantiomers [D]. Nanjing: Nanjing Agricultural University, 2019.
[91] 安雪花, 李冬雪, 代德茂, 等. 丁氟螨酯及其代谢物对大型溞的毒性效应[J]. 浙江农业学报, 2022, 34(3): 557-565.
An X H, Li D X, Dai D M, et al.Acute toxicity of cyflumetofen and its metabolites to Daphnia magna Straus[J]. Acta Agriculturae Zhejiangensis, 2022, 34(3): 557-565.
[92] 张召贤. 手性杀菌剂丙硫菌唑及其代谢物立体选择性研究[D]. 南京: 南京农业大学, 2020.
Zhang Z X.Study on the enantioselectivity of chiral fungicide prothioconazole and its metabolite [D]. Nanjing: Nanjing Agricultural University, 2020.
[93] 姚国君. 顺式氯氰菊酯及其代谢物的环境行为、生物毒性及其污染修复[D]. 北京: 中国农业大学, 2017.
Yao G J.Study on environmental behavior, biotoxicity and pollution remediation of alpha-cypermethrin and its metabolites [D]. Beijing: China Agricultural University, 2017.
[94] Li H X, Zhong Q, Wang M, et al.Residue degradation, transfer and risk assessment of pyriproxyfen and its metabolites from tea garden to cup by ultra performance liquid chromatography tandem mass spectrometry[J]. Journal of the Science of Food and Agriculture, 2022, 102(10): 3983-3993.
[95] 秦立新, 黄文源, 张盈, 等. 啶虫脒和吡丙醚在茶叶中的残留行为与膳食风险评估[J]. 农药, 2023, 62(3): 200-205.
Qin L X, Huang W Y, Zhang Y, et al.Residue behavior and dietary risk assessment of acetamiprid and pyriproxyfen in tea[J]. Agrochemicals, 2023, 62(3): 200-205.
[96] Liu R, Deng Y, Zhang W G, et al.Risk assessment of the chiral fungicide triticonazole: enantioselective effects, toxicity, and fate[J]. Journal of Agricultural and Food Chemistry, 2022, 70(8): 2712-2721.
[97] 孙彦. 9种手性农药的人体饮食暴露途径与残留特征研究[D]. 杭州: 浙江大学, 2019.
Sun Y.Study on dietary dietary exposure and residual characteristics of 9 chiral pesticides in human body [D]. Hangzhou: Zhejiang University, 2019.
[98] 姚小珊. 四种典型手性农药在全国土壤及人体尿液中对映体残留分析[D]. 武汉: 中南民族大学, 2019.
Yao X S.Enantiomer-specific residues of four typical chiral pesticides in agricultural soil across China and urine in human [D]. Wuhan: South-Central University for Nationalities, 2019.
[99] 顾元琳. 手性烯唑醇在四种水果中的对映体选择性降解、残留及风险评估[D]. 哈尔滨: 东北农业大学, 2022.
Gu Y L.Enantioselective degradation, residue, and risk assessment of chiral diniconazole in four kinds of fruits [D]. Haerbin: Northeast Agricultural University, 2022.
[100] 王微, 鄢人雨, 兰吉玉, 等. 黔东南州茶叶农药残留膳食摄入风险评估[J]. 茶叶科学, 2019, 39(5): 567-575.
Wang W, Yan R Y, Lan J Y, et al.Dietary intake risk assessment of pesticide residues in tea in Qiandongnan Prefecture[J]. Journal of Tea Science, 2019, 39(5): 567-575.
[101] 聂敏, 黄文源, 张盈, 等. 贵州省茶叶中3种拟除虫菊酯类农药残留及膳食风险评估[J]. 农药, 2023, 62(4): 272-276.
Nie M, Huang W Y, Zhang Y, et al.Residues and dietary risk assessment of 3 pyrethroid pesticides in tea in Guizhou Province[J]. Agrochemicals, 2023, 62(4): 272-276.
[102] 朱盼, 万欢, 黄芮, 等. 广东省本地产茶叶农药多残留累积风险评估[J]. 中国食品卫生杂志, 2022, 34(2): 308-314.
Zhu P, Wan H, Huang R, et al.Cumulative intake risk assessment of multi-pesicidies in local tea samples in Guangdong Province[J]. Chinese Journal of Food Hygiene, 2022, 34(2): 308-314.